Synthesis and crystal structure of the new uranyl selenite-selenate with melamine [(UO2)(SeO4)(H2SeO3)][(SeO4)(C3H8N6)]
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| RMS-DPI code: |
2012-1-179-0 |
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| Scientific session: |
F1. Mineralogical crystallogrpaphy and crystal chemistry |
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| Author listing: |
Tyshchenko D.V., Gurzhiy V.V., Krivovichev S.V. |
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| Principal author: |
Tyshchenko Darya Valer\'evna |
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| Language: |
Russian |
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Abstract - Summary
(short description): | |
| Single crystals of [(UO2)(SeO4)(H2SeO3)][(SeO4)(C3H8N6)] (1) were prepared by evaporation from 2 ml aqueous solution of uranyl nitrate, melamine and selenic acid. The unit cell parameters were determined by the least squares method. Compound (1) has a monoclinic symmetry, space group P21/c, a = 16.247(4) Å, b = 8.680(2) Å, c = 13.347(3)Å, = 90.615(5) o, V = 1882.1(8) Å3. The crystal structure was solved by direct methods from X-ray diffraction data and refined by the least-squares method to R1 = 0.0317 (wR2 = 0.0388) for 4068 reflections with |Fo| ≥ 4σF. |
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| Date of presentation: |
09/10/2012 |
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| Presentation Place: |
Mining University, foyer of the Assembly Hall |
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| RMS-DPI code: |
2012-1-179-0 |
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Proceeedings volume
in the RMS catalogue: | Mineralogy in à whole space of the word. |
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File of proceedings
(PDF): |
216 K
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| Status: |
printed |
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| Accepted: |
28/08/2012 |
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| Published on-line: |
05/11/2012 |
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| Permanent address of publication: |
http://www.minsoc.ru/2012-1-179-0/ |
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| Contact author(s): |
Tyshchenko, Darya Valer'evna |
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