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Fedorov session 2016
Saint Petersburg, Russia
11-12 October 2016
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Synthesis and crystal structure determination of the new copper diphosphate Cs2Cu(P2O7)

RMS-DPI code:  2016-1-35-0
Scientific session:  1. Mineralogical crystallography, crystal chemistry and new minerals
Author listing:  Chernyatieva A., Mannasova A.Z., Krivovichev S.V.
Principal author:  Chernyatieva Anastasiya Petrovna
Language:  Russian
Abstract - Summary 
(short description):
A crystal chemical study has allowed us to identify new phosphate. Single crystals of Cs2CuP2O7 have been prepared by high-temperature solid-state reactions. Mixture of CsNO3, CuSO4x5H2O and (NH4)4(P2O7) taken in stoichiometric proportion 3:1:1 was grounded and loaded into a corun-dum crucible. The crystal structure of Cs2CuP2O7 (monoclinic, Cc, a = 7.460(6), b = 12.973(10), c = 9.980(8) Å, β = 111.95(2), V = 895.8(12) Å3) prepared by solid-state reactions is based upon open framework formed by corner sharing between CuO4 distorted squares and P2O7 groups.
Keywords: crystal chemistry, crystal structure, mixed anion radicals, high-temperature synthesis, open framework structure; diamond net
 
Date of presentation:  11/10/2016
Presentation Place:  Mining University, foyer of the Assembly Hall
 
RMS-DPI code:  2016-1-35-0
File of proceedings 
(PDF): 
 113 K
Status:  preprint
Revised:  05/09/2016
Accepted:  05/09/2016
Contact author(s):  Chernyatieva, Anastasiya Petrovna
 

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